3ZKV
Importin13 cytosolic state
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | SLS BEAMLINE X10SA |
| Synchrotron site | SLS |
| Beamline | X10SA |
| Temperature [K] | 100 |
| Detector technology | CCD |
| Collection date | 2007-05-20 |
| Detector | MARRESEARCH |
| Spacegroup name | P 43 21 2 |
| Unit cell lengths | 167.720, 167.720, 95.630 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 46.517 - 3.000 |
| R-factor | 0.2738 |
| Rwork | 0.272 |
| R-free | 0.31080 |
| Structure solution method | MOLECULAR REPLACEMENT |
| Starting model (for MR) | 2x1g |
| RMSD bond length | 0.004 |
| RMSD bond angle | 0.809 |
| Data reduction software | XDS |
| Data scaling software | XSCALE |
| Phasing software | PHASER (MR) |
| Refinement software | PHENIX ((PHENIX.REFINE)) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 100.000 | 3.100 |
| High resolution limit [Å] | 3.000 | 3.000 |
| Rmerge | 0.160 | 1.170 |
| Number of reflections | 27903 | |
| <I/σ(I)> | 10.7 | 2.28 |
| Completeness [%] | 99.9 | 100 |
| Redundancy | 14.9 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 |
