3ZKR
X-ray structure of a pentameric ligand gated ion channel from Erwinia chrysanthemi (ELIC) in complex with bromoform
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | SLS BEAMLINE X06DA |
| Synchrotron site | SLS |
| Beamline | X06DA |
| Temperature [K] | 100 |
| Collection date | 2011-09-10 |
| Spacegroup name | P 1 21 1 |
| Unit cell lengths | 105.109, 266.248, 110.746 |
| Unit cell angles | 90.00, 109.78, 90.00 |
Refinement procedure
| Resolution | 44.083 - 3.649 |
| R-factor | 0.2305 |
| Rwork | 0.229 |
| R-free | 0.26390 |
| Structure solution method | MOLECULAR REPLACEMENT |
| RMSD bond length | 0.008 |
| RMSD bond angle | 1.335 |
| Refinement software | PHENIX ((PHENIX.REFINE)) |
Data quality characteristics
| Overall | |
| Low resolution limit [Å] | 44.080 |
| High resolution limit [Å] | 3.650 |
| Rmerge | 0.110 |
| Number of reflections | 62852 |
| <I/σ(I)> | 9.5 |
| Completeness [%] | 98.9 |
| Redundancy | 3.8 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 |
