3ZIL

Structure of the Wpl1 protein

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	ROTATING ANODE
Temperature [K]	100
Spacegroup name	I 1 2 1
Unit cell lengths	97.402, 35.207, 117.381
Unit cell angles	90.00, 101.89, 90.00

Refinement procedure

Resolution	29.120 - 2.012
R-factor	0.20204
Rwork	0.200
R-free	0.24567
Structure solution method	OTHER
Starting model (for MR)	NONE
RMSD bond length	0.020
RMSD bond angle	2.030
Refinement software	REFMAC (5.6)

Data quality characteristics

	Overall
Low resolution limit [Å]	30.000
High resolution limit [Å]	2.000
Rmerge	0.080
Number of reflections	26061
<I/σ(I)>	12.3
Completeness [%]	98.7
Redundancy	3.6

Crystallization Conditions

crystal ID	method	pH	temperature	details
1