3ZI0
Structure of Mycobacterium tuberculosis DXR in complex with a fosmidomycin analogue
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | ESRF BEAMLINE ID14-4 |
| Synchrotron site | ESRF |
| Beamline | ID14-4 |
| Temperature [K] | 110 |
| Detector technology | CCD |
| Collection date | 2011-03-31 |
| Detector | ADSC QUANTUM 315r |
| Spacegroup name | P 1 21 1 |
| Unit cell lengths | 67.447, 68.707, 85.700 |
| Unit cell angles | 90.00, 107.34, 90.00 |
Refinement procedure
| Resolution | 81.800 - 1.900 |
| R-factor | 0.20624 |
| Rwork | 0.205 |
| R-free | 0.23132 |
| Structure solution method | MOLECULAR REPLACEMENT |
| RMSD bond length | 0.007 |
| RMSD bond angle | 1.141 |
| Data reduction software | MOSFLM |
| Data scaling software | SCALA |
| Phasing software | PHASER |
| Refinement software | REFMAC (5.6.0117) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 81.800 | 2.000 |
| High resolution limit [Å] | 1.900 | 1.900 |
| Rmerge | 0.090 | 0.490 |
| Number of reflections | 58880 | |
| <I/σ(I)> | 12.2 | 3.2 |
| Completeness [%] | 99.7 | 99.9 |
| Redundancy | 6.6 | 6.8 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 |
