3ZFX
Crystal structure of EphB1
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | ESRF BEAMLINE ID14 |
| Synchrotron site | ESRF |
| Beamline | ID14 |
| Temperature [K] | 100 |
| Detector technology | CCD |
| Collection date | 2009-05-20 |
| Detector | MARRESEARCH |
| Spacegroup name | P 32 |
| Unit cell lengths | 195.980, 195.980, 60.242 |
| Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
| Resolution | 15.000 - 2.500 |
| R-factor | 0.18982 |
| Rwork | 0.188 |
| R-free | 0.21669 |
| Structure solution method | MOLECULAR REPLACEMENT |
| RMSD bond length | 0.012 |
| RMSD bond angle | 1.301 |
| Data reduction software | XDS |
| Data scaling software | SCALA |
| Phasing software | PHASER |
| Refinement software | REFMAC (5.6.0117) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 49.110 | 2.640 |
| High resolution limit [Å] | 2.500 | 2.500 |
| Rmerge | 0.150 | 0.600 |
| Number of reflections | 89433 | |
| <I/σ(I)> | 8.3 | 2.8 |
| Completeness [%] | 100.0 | 100 |
| Redundancy | 5.2 | 4.8 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 |
