3ZF8

Crystal structure of Saccharomyces cerevisiae Mnn9 in complex with GDP and Mn.

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	ESRF BEAMLINE ID14-4
Synchrotron site	ESRF
Beamline	ID14-4
Temperature [K]	100
Detector technology	CCD
Detector	ADSC QUANTUM 315
Spacegroup name	P 65 2 2
Unit cell lengths	57.090, 57.090, 330.910
Unit cell angles	90.00, 90.00, 120.00

Refinement procedure

Resolution	55.150 - 1.980
R-factor	0.19066
Rwork	0.190
R-free	0.23920
Structure solution method	OTHER
Starting model (for MR)	NONE
RMSD bond length	0.012
RMSD bond angle	1.429
Refinement software	REFMAC (5.6.0117)

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	55.000	2.200
High resolution limit [Å]	2.000	2.000
Rmerge	0.150
Number of reflections	23775
<I/σ(I)>	11.8
Completeness [%]	100.0	100
Redundancy	9.7

Crystallization Conditions

crystal ID	method	pH	temperature	details
1