3ZEW
Crystal structure of EphB4 in complex with staurosporine
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | ROTATING ANODE |
| Source details | RIGAKU MICROMAX-007 |
| Temperature [K] | 100 |
| Detector technology | CCD |
| Collection date | 2009-07-19 |
| Detector | RIGAKU SATURN |
| Spacegroup name | P 1 21 1 |
| Unit cell lengths | 52.170, 88.710, 80.780 |
| Unit cell angles | 90.00, 103.05, 90.00 |
Refinement procedure
| Resolution | 15.000 - 2.500 |
| R-factor | 0.2401 |
| Rwork | 0.238 |
| R-free | 0.28160 |
| Structure solution method | MOLECULAR REPLACEMENT |
| RMSD bond length | 0.009 |
| RMSD bond angle | 1.030 |
| Data reduction software | d*TREK |
| Data scaling software | DTSCALE |
| Phasing software | PHASER |
| Refinement software | BUSTER (2.11.5) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 33.420 | 2.590 |
| High resolution limit [Å] | 2.500 | 2.500 |
| Rmerge | 0.110 | 0.330 |
| Number of reflections | 22752 | |
| <I/σ(I)> | 6.3 | 2.4 |
| Completeness [%] | 91.3 | 90.3 |
| Redundancy | 3.22 | 3.33 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 |
