3WUL
Crystal structure of hen egg-white lysozyme
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | FREE ELECTRON LASER |
| Source details | SACLA BEAMLINE BL3 |
| Synchrotron site | SACLA |
| Beamline | BL3 |
| Temperature [K] | 293 |
| Detector technology | CCD |
| Collection date | 2013-12-09 |
| Detector | MPCCD octal |
| Wavelength(s) | 1.23 |
| Spacegroup name | P 43 21 2 |
| Unit cell lengths | 79.000, 79.000, 38.000 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 19.160 - 2.000 |
| R-factor | 0.2076 |
| Rwork | 0.207 |
| R-free | 0.22977 |
| Structure solution method | FOURIER SYNTHESIS |
| RMSD bond length | 0.022 |
| RMSD bond angle | 1.512 |
| Data reduction software | CrystFEL |
| Data scaling software | XDS |
| Phasing software | REFMAC |
| Refinement software | REFMAC (5.5.0109) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 30.000 | 2.040 |
| High resolution limit [Å] | 2.000 | 2.000 |
| Number of reflections | 8545 | |
| Completeness [%] | 99.9 | 100 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | batch | 3 | 293 | sodium chloride, PEG 6000, pH 3.0, batch, temperature 293K |
