3WQL

Crystal structure of Rv3378c with Mg2+ and PPi

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	NSRRC BEAMLINE BL13C1
Synchrotron site	NSRRC
Beamline	BL13C1
Temperature [K]	100
Detector technology	CCD
Collection date	2011-11-06
Detector	ADSC QUANTUM 315r
Wavelength(s)	1
Spacegroup name	C 1 2 1
Unit cell lengths	208.420, 56.525, 114.435
Unit cell angles	90.00, 90.28, 90.00

Refinement procedure

Resolution	25.000 - 2.100
Rwork	0.198
R-free	0.23900
Structure solution method	MOLECULAR REPLACEMENT
Starting model (for MR)	3wqk
Data reduction software	HKL-2000
Data scaling software	HKL-2000
Phasing software	PHASER
Refinement software	CNS (1.2)

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	25.000	2.200
High resolution limit [Å]	2.100	2.100
Rmerge	0.065	0.416
Number of reflections	77301
<I/σ(I)>		2.3
Completeness [%]	98.1	85.6
Redundancy	3.9	2.7

Crystallization Conditions

crystal ID	method	pH	temperature	details
1