3WQA
Acinetobacter sp. Tol 5 AtaA YDD-DALL3 domains in C-terminal stalk fused to GCN4 adaptors (CstalkC1ii)
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SLS BEAMLINE X10SA |
Synchrotron site | SLS |
Beamline | X10SA |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2013-06-20 |
Detector | PSI PILATUS 6M |
Wavelength(s) | 1.0 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 86.110, 43.680, 95.564 |
Unit cell angles | 90.00, 111.97, 90.00 |
Refinement procedure
Resolution | 38.322 - 2.401 |
R-factor | 0.2179 |
Rwork | 0.213 |
R-free | 0.30700 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 2yo2 |
RMSD bond length | 0.008 |
RMSD bond angle | 1.089 |
Data reduction software | XDS |
Data scaling software | XSCALE |
Phasing software | MOLREP |
Refinement software | PHENIX (1.8.1_1168) |
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 88.560 | 2.540 | |
High resolution limit [Å] | 2.400 | 7.080 | 2.400 |
Rmerge | 0.048 | 0.641 | |
Rmeas | 0.058 | 0.765 | |
Number of reflections | 26029 | 1075 | 4049 |
<I/σ(I)> | 18.53 | 1.83 | |
Completeness [%] | 98.9 | 97.5 | 96.8 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 6.5 | 298 | 67mM MES, 0.67M Ammonium sulfate, pH 6.5, VAPOR DIFFUSION, HANGING DROP, temperature 298K |