3WPI

Crystal structure of mouse TLR9 in complex with inhibitory DNA_super

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	PHOTON FACTORY BEAMLINE AR-NE3A
Synchrotron site	Photon Factory
Beamline	AR-NE3A
Temperature [K]	100
Detector technology	CCD
Collection date	2012-12-08
Detector	ADSC QUANTUM 270
Wavelength(s)	1.0000
Spacegroup name	C 1 2 1
Unit cell lengths	137.330, 129.720, 71.360
Unit cell angles	90.00, 92.17, 90.00

Refinement procedure

Resolution	36.341 - 2.246
R-factor	0.2231
Rwork	0.221
R-free	0.25400
Structure solution method	MOLECULAR REPLACEMENT
RMSD bond length	0.004
RMSD bond angle	0.985
Data reduction software	MOSFLM
Data scaling software	SCALA
Phasing software	MOLREP
Refinement software	PHENIX (1.8.1_1168)

Data quality characteristics

	Overall
Low resolution limit [Å]	57.600
High resolution limit [Å]	2.246
Number of reflections	57648

Crystallization Conditions

crystal ID	method	pH	temperature	details
1