3WHD

C-type lectin, human MCL

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	SPRING-8 BEAMLINE BL32XU
Synchrotron site	SPring-8
Beamline	BL32XU
Temperature [K]	100
Detector technology	CCD
Collection date	2011-04-12
Wavelength(s)	1.0
Spacegroup name	I 2 2 2
Unit cell lengths	85.190, 96.056, 104.826
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	40.483 - 2.290
R-factor	0.1778
Rwork	0.176
R-free	0.21800
Structure solution method	MOLECULAR REPLACEMENT
RMSD bond length	0.009
RMSD bond angle	1.171
Data reduction software	HKL-2000
Data scaling software	HKL-2000
Phasing software	MOLREP
Refinement software	PHENIX ((phenix.refine: 1.8.2_1309))

Data quality characteristics

	Overall
Low resolution limit [Å]	40.483
High resolution limit [Å]	2.290
Rmerge	0.141
Number of reflections	19569
<I/σ(I)>	8.65
Completeness [%]	100.0
Redundancy	7.2

Crystallization Conditions

crystal ID	method	pH	temperature	details
1