3VTU
Crystal structure of human LC3B_2-119
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | PHOTON FACTORY BEAMLINE AR-NW12A |
Synchrotron site | Photon Factory |
Beamline | AR-NW12A |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2010-11-18 |
Detector | ADSC QUANTUM 210 |
Wavelength(s) | 1.0000 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 34.680, 53.550, 61.020 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 22.910 - 1.600 |
R-factor | 0.1835 |
Rwork | 0.181 |
R-free | 0.23121 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 3eci |
RMSD bond length | 0.027 |
RMSD bond angle | 2.364 |
Data reduction software | MOSFLM |
Data scaling software | SCALA |
Phasing software | MOLREP |
Refinement software | REFMAC (5.5.0109) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 22.910 | 1.690 |
High resolution limit [Å] | 1.600 | 1.600 |
Rmerge | 0.063 | 0.373 |
Number of reflections | 15380 | |
<I/σ(I)> | 22.1 | 5.5 |
Completeness [%] | 99.0 | 98.5 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 5.6 | 293 | 2.0M Ammonium sulfate, 0.1M Tri-sodium citrate, 0.2M Potassium sodium tartrate, pH 5.6, VAPOR DIFFUSION, SITTING DROP, temperature 293K |