3VJJ

Crystal Structure Analysis of the P9-1

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	SPRING-8 BEAMLINE BL44XU
Synchrotron site	SPring-8
Beamline	BL44XU
Temperature [K]	100
Detector technology	CCD
Collection date	2010-10-11
Detector	ADSC QUANTUM 210
Wavelength(s)	0.9
Spacegroup name	P 4 21 2
Unit cell lengths	127.284, 127.284, 143.227
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	42.176 - 3.000
R-factor	0.2449
Rwork	0.243
R-free	0.29280
Structure solution method	MAD
RMSD bond length	0.013
RMSD bond angle	1.654
Data reduction software	HKL-2000
Data scaling software	HKL-2000
Phasing software	SOLVE
Refinement software	PHENIX ((phenix.refine: 1.7_650))

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	44.800
High resolution limit [Å]	3.000	3.000
Number of reflections	24512
Completeness [%]	100.0	100

Crystallization Conditions

crystal ID	method	pH	temperature	details
1
1