3V55
Human MALT1 (334-719) in its ligand free form
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | SLS BEAMLINE X10SA |
| Synchrotron site | SLS |
| Beamline | X10SA |
| Temperature [K] | 100 |
| Detector technology | PIXEL |
| Collection date | 2011-07-10 |
| Detector | PSI PILATUS 6M |
| Wavelength(s) | 1 |
| Spacegroup name | C 1 2 1 |
| Unit cell lengths | 96.650, 67.250, 58.040 |
| Unit cell angles | 90.00, 97.31, 90.00 |
Refinement procedure
| Resolution | 41.330 - 1.810 |
| R-factor | 0.1979 |
| Rwork | 0.196 |
| R-free | 0.23820 |
| Structure solution method | FOURIER METHODS |
| RMSD bond length | 0.010 |
| RMSD bond angle | 1.180 |
| Data reduction software | XDS |
| Data scaling software | XSCALE |
| Phasing software | PHASER |
| Refinement software | BUSTER (2.11.2) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 41.330 | 1.813 |
| High resolution limit [Å] | 1.807 | 1.807 |
| Rmerge | 0.043 | 0.458 |
| Number of reflections | 33103 | |
| <I/σ(I)> | 15.4 | 2.3 |
| Completeness [%] | 97.7 | 97.6 |
| Redundancy | 3.3 | 3.2 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION | 298 | 0.2M magnesium formate, 20% PEG3350, VAPOR DIFFUSION, temperature 298K |
