3UZD
Crystal structure of 14-3-3 GAMMA
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 19-ID |
Synchrotron site | APS |
Beamline | 19-ID |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2010-08-18 |
Detector | ADSC QUANTUM 315 |
Wavelength(s) | 0.97924 |
Spacegroup name | I 2 2 2 |
Unit cell lengths | 60.511, 79.230, 122.232 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 66.480 - 1.860 |
R-factor | 0.196 |
Rwork | 0.194 |
R-free | 0.23000 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 2b05 |
RMSD bond length | 0.017 |
RMSD bond angle | 1.526 |
Data scaling software | SCALEPACK |
Phasing software | PHASER |
Refinement software | REFMAC (5.5.0102) |
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 66.480 | 50.000 | 1.890 |
High resolution limit [Å] | 1.860 | 5.050 | 1.860 |
Rmerge | 0.050 | 0.023 | 0.845 |
Number of reflections | 24650 | ||
<I/σ(I)> | 15.7 | ||
Completeness [%] | 98.3 | 99.2 | 96.1 |
Redundancy | 7.1 | 6.7 | 7.1 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 291 | 0.3M Mg (OAc)2, 20% PEG3350, vapor diffusion, hanging drop, temperature 291K |