Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | APS BEAMLINE 21-ID-F |
| Synchrotron site | APS |
| Beamline | 21-ID-F |
| Temperature [K] | 100 |
| Detector technology | CCD |
| Collection date | 2010-07-08 |
| Detector | MARMOSAIC 225 mm CCD |
| Wavelength(s) | 0.979 |
| Spacegroup name | C 1 2 1 |
| Unit cell lengths | 119.687, 45.334, 68.607 |
| Unit cell angles | 90.00, 97.95, 90.00 |
Refinement procedure
| Resolution | 50.000 - 1.680 |
| R-factor | 0.1759 |
| Rwork | 0.174 |
| R-free | 0.21320 |
| Structure solution method | SAD |
| RMSD bond length | 0.013 |
| RMSD bond angle | 1.591 |
| Data reduction software | HKL-2000 |
| Data scaling software | HKL-2000 |
| Phasing software | HKL-3000 (SHELXC/D/E) |
| Refinement software | REFMAC (5.6.0117) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 50.000 | 1.690 |
| High resolution limit [Å] | 1.680 | 1.680 |
| Rmerge | 0.039 | 0.398 |
| Number of reflections | 41594 | |
| <I/σ(I)> | 24.38 | 2.2 |
| Completeness [%] | 99.9 | 99.4 |
| Redundancy | 4.1 | 4 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, HANGING DROP | 5.5 | 293 | 25% PEG 3350, 0.2M NaCl, 0.1M Bis-Tris, 2% Hexandiol, pH 5.5, VAPOR DIFFUSION, HANGING DROP, temperature 293K |
