3UT8

Structural view of a non Pfam singleton and crystal packing analysis

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	ROTATING ANODE
Source details	RIGAKU MICROMAX-007
Collection date	2011-02-22
Wavelength(s)	1.541
Spacegroup name	P 21 21 21
Unit cell lengths	50.105, 63.885, 96.909
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	27.148 - 2.168
R-factor	0.223
Rwork	0.223
R-free	0.22660
RMSD bond length	0.008
RMSD bond angle	1.058
Data reduction software	HKL-2000
Data scaling software	HKL-2000
Phasing software	PHASES
Refinement software	PHENIX ((phenix.refine: 1.7.2_869))

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	30.580	2.250
High resolution limit [Å]	2.168	2.170
Number of reflections	16720
Completeness [%]	97.7	97.7

Crystallization Conditions

crystal ID	method	pH	temperature	details
1