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3UT1

Crystal structure of the 3-MBT repeat domain of L3MBTL3

Experimental procedure
Experimental methodSINGLE WAVELENGTH
Source typeSYNCHROTRON
Source detailsCHESS BEAMLINE F1
Synchrotron siteCHESS
BeamlineF1
Temperature [K]100
Detector technologyCCD
Collection date2011-10-19
DetectorADSC QUANTUM 270
Wavelength(s)0.9179
Spacegroup nameC 1 2 1
Unit cell lengths92.287, 70.619, 58.574
Unit cell angles90.00, 119.95, 90.00
Refinement procedure
Resolution44.761 - 2.050
R-factor0.224
Rwork0.222
R-free0.26700
Structure solution methodMOLECULAR REPLACEMENT
Starting model (for MR)based on unpublished model of L3MBTL1 itself based on molecular replacement with coordinates from PDB entry 1OYX
RMSD bond length0.011
RMSD bond angle1.309
Data reduction softwareDENZO
Data scaling softwareSCALEPACK
Phasing softwarePHASER
Refinement softwareREFMAC (5.6.0117)
Data quality characteristics
 OverallInner shellOuter shell
Low resolution limit [Å]50.00050.0002.120
High resolution limit [Å]2.0504.4202.050
Rmerge0.1300.0570.859
Number of reflections20483
<I/σ(I)>6.1
Completeness [%]99.999.899.5
Redundancy5.45.44.5
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
1VAPOR DIFFUSION5.529127% PEG-3350, 0.1M ammonium sulfate, 0.2M cobaltous chloride, 0.1M Bis-tris, pH 5.5, vapor diffusion, temperature 291K

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