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3UHK

HBI (K96R) without ligand bound

Experimental procedure
Experimental methodSINGLE WAVELENGTH
Source typeROTATING ANODE
Source detailsRIGAKU RU200
Temperature [K]298
Detector technologyIMAGE PLATE
Collection date2000-09-23
DetectorRIGAKU RAXIS IIC
Wavelength(s)1.5418
Spacegroup nameP 1 21 1
Unit cell lengths83.880, 44.040, 87.230
Unit cell angles90.00, 115.33, 90.00
Refinement procedure
Resolution30.910 - 2.000
R-factor0.194
Rwork0.194
R-free0.22100
Structure solution methodMOLECULAR REPLACEMENT
Starting model (for MR)3sdh
RMSD bond length0.006
RMSD bond angle1.200
Data reduction softwareDENZO
Data scaling softwareSCALEPACK
Phasing softwareCNS
Refinement softwareCNS
Data quality characteristics
 OverallOuter shell
Low resolution limit [Å]40.0002.070
High resolution limit [Å]2.0002.000
Rmerge0.0930.278
Number of reflections36200
<I/σ(I)>10.43.8
Completeness [%]91.894.9
Redundancy2.9
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
1MICROBATCH7.52962.1-2.3 M phosphate buffer, pH 7.5, MICROBATCH, temperature 296K

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