3U65
The Crystal Structure of Tat-P(T) (Tp0957)
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 19-ID |
Synchrotron site | APS |
Beamline | 19-ID |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2011-06-16 |
Detector | ADSC QUANTUM 315r |
Wavelength(s) | 0.97818 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 37.693, 148.038, 59.138 |
Unit cell angles | 90.00, 97.11, 90.00 |
Refinement procedure
Resolution | 37.768 - 1.400 |
R-factor | 0.1792 |
Rwork | 0.178 |
R-free | 0.20130 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.009 |
RMSD bond angle | 1.194 |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Phasing software | PHASER |
Refinement software | PHENIX (1.7.1_743) |
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 50.000 | 50.000 | 1.420 |
High resolution limit [Å] | 1.400 | 3.800 | 1.400 |
Rmerge | 0.037 | 0.023 | 0.566 |
Number of reflections | 125807 | ||
<I/σ(I)> | 15.5 | ||
Completeness [%] | 99.8 | 97.3 | 99.7 |
Redundancy | 4.1 | 4.1 | 3.6 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION | 7.5 | 293 | 20% PEG 3350, 0.2 M KSCN, pH 7.5, VAPOR DIFFUSION, temperature 293K |