3TXT
Crystal structure of GlpG in complex with inhibitor DFP
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU |
Temperature [K] | 100 |
Detector technology | IMAGE PLATE |
Collection date | 2011-01-20 |
Detector | RIGAKU RAXIS |
Wavelength(s) | 1.54 |
Spacegroup name | H 3 2 |
Unit cell lengths | 109.667, 109.667, 125.097 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 23.327 - 2.300 |
R-factor | 0.2199 |
Rwork | 0.219 |
R-free | 0.23840 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.007 |
RMSD bond angle | 0.985 |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Phasing software | REFMAC |
Refinement software | PHENIX ((phenix.refine: 1.7.1_743)) |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 40.000 |
High resolution limit [Å] | 2.300 |
Number of reflections | 12996 |
Completeness [%] | 99.0 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION | 7 | 298 | 3M NaCl, 0.1 M bis-tris propane, pH7, VAPOR DIFFUSION, temperature 298K |