3TVY
Structural Analysis of Adhesive Tip pilin, GBS104 from Group B Streptococcus agalactiae
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU |
Temperature [K] | 100 |
Detector technology | IMAGE PLATE |
Collection date | 2010-01-07 |
Detector | RIGAKU RAXIS IV |
Wavelength(s) | 1.5418 |
Spacegroup name | P 21 21 2 |
Unit cell lengths | 74.749, 101.290, 52.665 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 35.064 - 2.000 |
R-factor | 0.21214 |
Rwork | 0.210 |
R-free | 0.25111 |
Structure solution method | SAD |
RMSD bond length | 0.014 |
RMSD bond angle | 1.468 |
Data reduction software | d*TREK |
Data scaling software | d*TREK |
Phasing software | PHENIX |
Refinement software | REFMAC (5.5.0109) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 35.064 | 2.070 |
High resolution limit [Å] | 2.000 | 2.000 |
Rmerge | 0.120 | 0.450 |
Number of reflections | 27094 | |
<I/σ(I)> | 9.3 | 3.1 |
Completeness [%] | 97.7 | 94.4 |
Redundancy | 5.8 | 5.2 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 7.5 | 295 | 20% PEG8000, 0.1 M HEPES, pH 7.5, VAPOR DIFFUSION, HANGING DROP, temperature 295K |