3TUX
Crystal structure of RtcA.ATP.Mn ternary complex
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | NSLS BEAMLINE X25 |
Synchrotron site | NSLS |
Beamline | X25 |
Temperature [K] | 130 |
Detector technology | PIXEL |
Collection date | 2011-04-30 |
Detector | DECTRIS PILATUS 6M |
Wavelength(s) | 0.9499 |
Spacegroup name | P 21 21 2 |
Unit cell lengths | 69.530, 83.060, 52.080 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 26.658 - 1.850 |
R-factor | 0.1886 |
Rwork | 0.185 |
R-free | 0.25160 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 3kgd |
RMSD bond length | 0.007 |
RMSD bond angle | 1.164 |
Data reduction software | MOSFLM |
Data scaling software | SCALA |
Phasing software | PHENIX |
Refinement software | PHENIX ((phenix.refine: dev_833)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 27.310 | 1.950 |
High resolution limit [Å] | 1.850 | 1.850 |
Number of reflections | 25908 | |
Completeness [%] | 98.5 | 96.8 |
Redundancy | 5.7 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 6.5 | 293 | 28% PEG5000 MME, 150 mM Ammonium sulfate, 100 mM MES pH6.5, 10 mM ATP, 20 mM Manganese chloride, VAPOR DIFFUSION, HANGING DROP, temperature 293K |