3TRQ

Crystal structure of native rabbit skeletal calsequestrin

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	ALS BEAMLINE 8.2.1
Synchrotron site	ALS
Beamline	8.2.1
Detector technology	CCD
Detector	ADSC QUANTUM 315r
Spacegroup name	C 2 2 21
Unit cell lengths	59.271, 144.565, 111.170
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	30.704 - 1.760
R-factor	0.1798
Rwork	0.178
R-free	0.21340
Structure solution method	FOURIER SYNTHESIS
Starting model (for MR)	1a8y
RMSD bond length	0.012
RMSD bond angle	0.807
Refinement software	PHENIX ((phenix.refine: 1.6.1_357))

Data quality characteristics

	Overall
Low resolution limit [Å]	31.100
High resolution limit [Å]	1.760
Number of reflections	46768

Crystallization Conditions

crystal ID	method	pH	temperature	details
1
1