3TG7
Crystal structure of Adenovirus serotype 5 hexon at 1.6A resolution
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | DIAMOND BEAMLINE I02 |
| Synchrotron site | Diamond |
| Beamline | I02 |
| Detector technology | CCD |
| Collection date | 2010-10-21 |
| Detector | ADSC QUANTUM 4 |
| Wavelength(s) | 0.9763 |
| Spacegroup name | H 3 |
| Unit cell lengths | 149.150, 149.150, 126.690 |
| Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
| Resolution | 45.550 - 1.570 |
| R-factor | 0.18578 |
| Rwork | 0.184 |
| R-free | 0.22272 |
| Structure solution method | MOLECULAR REPLACEMENT |
| Starting model (for MR) | 1p30 |
| RMSD bond length | 0.028 |
| RMSD bond angle | 2.306 |
| Data reduction software | d*TREK |
| Data scaling software | d*TREK |
| Phasing software | PHASER |
| Refinement software | REFMAC (5.5.0102) |
Data quality characteristics
| Overall | |
| Low resolution limit [Å] | 45.550 |
| High resolution limit [Å] | 1.570 |
| Rmerge | 0.062 |
| Number of reflections | 138241 |
| Completeness [%] | 99.8 |
| Redundancy | 3.9 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, SITTING DROP | 6.5 | 291 | 14% PEG 6000 in Bis-tris propane buffer., pH 6.5, VAPOR DIFFUSION, SITTING DROP, temperature 291K |
