3TD4
Crystal structure of OmpA-like domain from Acinetobacter baumannii in complex with diaminopimelate
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | PHOTON FACTORY BEAMLINE BL-17A |
| Synchrotron site | Photon Factory |
| Beamline | BL-17A |
| Temperature [K] | 100 |
| Detector technology | CCD |
| Collection date | 2009-10-24 |
| Detector | ADSC QUANTUM 315r |
| Wavelength(s) | 0.98 |
| Spacegroup name | P 1 21 1 |
| Unit cell lengths | 57.873, 98.225, 98.438 |
| Unit cell angles | 90.00, 105.51, 90.00 |
Refinement procedure
| Resolution | 94.860 - 1.790 |
| R-factor | 0.18048 |
| Rwork | 0.179 |
| R-free | 0.21444 |
| Structure solution method | MOLECULAR REPLACEMENT |
| Starting model (for MR) | 3td3 |
| RMSD bond length | 0.029 |
| RMSD bond angle | 2.444 |
| Data reduction software | HKL-2000 |
| Data scaling software | HKL-2000 |
| Phasing software | MOLREP |
| Refinement software | REFMAC (5.5.0109) |
Data quality characteristics
| Overall | |
| Low resolution limit [Å] | 94.860 |
| High resolution limit [Å] | 1.790 |
| Number of reflections | 93970 |
| Completeness [%] | 99.1 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, HANGING DROP | 8 | 293 | 0.1M Ammonium tartrate, 15%-20% PEG3350, pH 8, VAPOR DIFFUSION, HANGING DROP, temperature 293K |
