3T7I
Crystal structure of Se-Met Rtt107p (residues 820-1070)
Experimental procedure
Experimental method | MAD |
Source type | SYNCHROTRON |
Source details | SSRF BEAMLINE BL17U |
Synchrotron site | SSRF |
Beamline | BL17U |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2010-09-13 |
Detector | MARMOSAIC 225 mm CCD |
Wavelength(s) | 0.9805, 0.9807, 0.9567 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 59.236, 74.636, 129.080 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 19.986 - 2.300 |
R-factor | 0.2055 |
Rwork | 0.203 |
R-free | 0.24810 |
Structure solution method | MAD |
RMSD bond length | 0.008 |
RMSD bond angle | 1.038 |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Phasing software | SOLVE (2.13) |
Refinement software | PHENIX (1.6.1_357) |
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 50.000 | 50.000 | 2.340 |
High resolution limit [Å] | 2.300 | 6.240 | 2.300 |
Rmerge | 0.106 | 0.063 | 0.313 |
Number of reflections | 26232 | ||
<I/σ(I)> | 11.5 | ||
Completeness [%] | 99.8 | 97.8 | 100 |
Redundancy | 12.2 | 11 | 11.7 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 7 | 283 | 17.5%(w/v) MPEG2000, 0.1M HEPES, 0.2M NaCl, pH 7.0, VAPOR DIFFUSION, HANGING DROP, temperature 283K |