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3SR9

Crystal structure of mouse PTPsigma

Experimental procedure
Experimental methodSINGLE WAVELENGTH
Source typeSYNCHROTRON
Source detailsSSRF BEAMLINE BL17U
Synchrotron siteSSRF
BeamlineBL17U
Temperature [K]100
Detector technologyCCD
Collection date2010-04-14
DetectorADSC QUANTUM 315r
Wavelength(s)1
Spacegroup nameP 61
Unit cell lengths94.653, 94.653, 124.201
Unit cell angles90.00, 90.00, 120.00
Refinement procedure
Resolution50.000 - 2.400
R-factor0.2347
Rwork0.233
R-free0.27180
Structure solution methodMOLECULAR REPLACEMENT
Starting model (for MR)2fh7
RMSD bond length0.007
RMSD bond angle0.973
Refinement softwareREFMAC (5.5.0102)
Data quality characteristics
 Overall
Low resolution limit [Å]50.000
High resolution limit [Å]2.400
Number of reflections22320
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
1VAPOR DIFFUSION727715% polyethylene glycol 3350, 0.08M malic acid, pH 7.0, VAPOR DIFFUSION, temperature 277K

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