3SQ1
RB69 DNA Polymerase Ternary Complex with dUpCpp Opposite dA
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 24-ID-C |
Synchrotron site | APS |
Beamline | 24-ID-C |
Temperature [K] | 110 |
Detector technology | CCD |
Collection date | 2011-02-12 |
Detector | APEX II CCD |
Wavelength(s) | 0.97918 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 75.101, 120.470, 130.561 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 88.540 - 1.820 |
R-factor | 0.18352 |
Rwork | 0.182 |
R-free | 0.21267 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.007 |
RMSD bond angle | 1.082 |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Phasing software | AMoRE |
Refinement software | REFMAC (5.5.0109) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 88.540 | 1.860 |
High resolution limit [Å] | 1.820 | 1.820 |
Number of reflections | 99798 | |
Completeness [%] | 94.7 | 97.3 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION | 6.5 | 298 | 150 mM calcium chloride, 15% w/v PEG350 MME, 100 mM sodium cacodylate, pH 6.5, VAPOR DIFFUSION, temperature 298K |