3S98
human IFNAR1
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | SSRL BEAMLINE BL9-1 |
| Synchrotron site | SSRL |
| Beamline | BL9-1 |
| Temperature [K] | 100 |
| Detector technology | CCD |
| Collection date | 2009-03-19 |
| Detector | ADSC QUANTUM 315r |
| Spacegroup name | P 21 21 21 |
| Unit cell lengths | 47.090, 86.180, 91.340 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 19.486 - 1.900 |
| Rwork | 0.210 |
| R-free | 0.23400 |
| Structure solution method | SIRAS |
| RMSD bond length | 0.023 |
| RMSD bond angle | 1.345 |
| Data reduction software | XDS |
| Data scaling software | XSCALE |
| Phasing software | autoSHARP |
| Refinement software | PHENIX |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 19.486 | 2.000 |
| High resolution limit [Å] | 1.900 | 1.900 |
| Number of reflections | 55817 | |
| <I/σ(I)> | 21.1 | 3.4 |
| Completeness [%] | 98.6 | 98.3 |
| Redundancy | 7.6 | 7.6 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | 298 | 20% (w/v) PEG 3350, VAPOR DIFFUSION, HANGING DROP, temperature 298K |
