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3S60

Structure of the cyanobacterial Oscillatoria Agardhii Agglutinin (OAA) in free state obtained at 25 degree Celsius

Experimental procedure
Experimental methodSINGLE WAVELENGTH
Source typeROTATING ANODE
Source detailsRIGAKU FR-E SUPERBRIGHT
Temperature [K]298
Detector technologyCCD
Collection date2010-10-01
DetectorRIGAKU SATURN 944+
Wavelength(s)1.54
Spacegroup nameP 21 21 21
Unit cell lengths39.467, 40.658, 70.374
Unit cell angles90.00, 90.00, 90.00
Refinement procedure
Resolution26.610 - 1.600
R-factor0.18706
Rwork0.182
R-free0.22793
Structure solution methodMOLECULAR REPLACEMENT
Starting model (for MR)3s5v
RMSD bond length0.022
RMSD bond angle1.933
Data reduction softwared*TREK
Data scaling softwared*TREK
Phasing softwarePHASER
Refinement softwareREFMAC (5.5.0044)
Data quality characteristics
 OverallOuter shell
Low resolution limit [Å]26.6101.660
High resolution limit [Å]1.6001.600
Rmerge0.0810.309
Number of reflections13272
<I/σ(I)>8.71.5
Completeness [%]95.091.5
Redundancy2.481.8
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
1VAPOR DIFFUSION, SITTING DROP82982.0 M (NH4)SO4 and 0.1 M Tris-HCl (pH 8.5), VAPOR DIFFUSION, SITTING DROP, temperature 298K

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