3RZS
Apis mellifera OBP14 in complex with Ta6Br14
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SOLEIL BEAMLINE PROXIMA 1 |
Synchrotron site | SOLEIL |
Beamline | PROXIMA 1 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2010-12-08 |
Detector | ADSC QUANTUM 315r |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 33.260, 38.030, 86.810 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 31.060 - 1.880 |
R-factor | 0.207 |
Rwork | 0.206 |
R-free | 0.22360 |
Structure solution method | SAD |
RMSD bond length | 0.011 |
RMSD bond angle | 1.440 |
Data reduction software | XDS |
Data scaling software | XSCALE |
Phasing software | SHARP |
Refinement software | BUSTER (2.9.2) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 33.300 | 1.980 |
High resolution limit [Å] | 1.880 | 1.880 |
Rmerge | 0.063 | 0.280 |
Number of reflections | 9512 | |
<I/σ(I)> | 20.2 | 5.7 |
Completeness [%] | 100.0 | 98.7 |
Redundancy | 8 | 7.2 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 9.8 | 293 | 1.8-1.9 M tri-sodium citrate, 25 mM CHES, pH 9.8, VAPOR DIFFUSION, SITTING DROP, temperature 293K |