3RT5
Lysozyme in 30% propanol
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU MICROMAX-007 HF |
Temperature [K] | 100 |
Detector technology | IMAGE PLATE |
Collection date | 2010-10-15 |
Detector | MAR scanner 345 mm plate |
Wavelength(s) | 1.5418 |
Spacegroup name | P 43 21 2 |
Unit cell lengths | 77.935, 77.935, 36.961 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 25.358 - 1.750 |
R-factor | 0.1842 |
Rwork | 0.183 |
R-free | 0.21370 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.023 |
RMSD bond angle | 1.033 |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Phasing software | PHASES |
Refinement software | PHENIX ((phenix.refine: 1.7_650)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 1.780 |
High resolution limit [Å] | 1.750 | 1.750 |
Rmerge | 0.038 | 0.096 |
Number of reflections | 12009 | |
<I/σ(I)> | 42.8 | 16 |
Completeness [%] | 99.4 | 100 |
Redundancy | 4.4 | 4.3 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 3.8 | 277 | 40mM Sodium Acetate, 150mM Sodium chloride, 30% 2-propanol, pH 3.8, VAPOR DIFFUSION, HANGING DROP, temperature 277K |