3RKW
Structural characterisation of staphylococcus aureus biotin protein ligase
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | AUSTRALIAN SYNCHROTRON BEAMLINE MX1 |
| Synchrotron site | Australian Synchrotron |
| Beamline | MX1 |
| Wavelength(s) | 1.0 |
| Spacegroup name | P 42 21 2 |
| Unit cell lengths | 94.598, 94.598, 130.626 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 39.553 - 2.500 |
| R-factor | 0.2155 |
| Rwork | 0.213 |
| R-free | 0.26270 |
| Starting model (for MR) | 3rir |
| RMSD bond length | 0.022 |
| RMSD bond angle | 2.030 |
| Data reduction software | MOSFLM |
| Data scaling software | SCALA |
| Refinement software | PHENIX ((phenix.refine: 1.6.4_486)) |
Data quality characteristics
| Overall | |
| Low resolution limit [Å] | 40.000 |
| High resolution limit [Å] | 2.500 |
| Number of reflections | 20973 |
| Completeness [%] | 98.2 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 |
