Experimental procedure
| Experimental method | MAD |
| Source type | SYNCHROTRON |
| Source details | ALS BEAMLINE 12.3.1 |
| Synchrotron site | ALS |
| Beamline | 12.3.1 |
| Detector technology | CCD |
| Collection date | 2005-12-16 |
| Detector | ADSC QUANTUM 315r |
| Wavelength(s) | 1.28279 |
| Spacegroup name | P 63 2 2 |
| Unit cell lengths | 96.700, 96.700, 114.300 |
| Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
| Resolution | 48.350 - 2.200 |
| R-factor | 0.219 |
| Rwork | 0.219 |
| R-free | 0.23500 |
| Structure solution method | MAD |
| RMSD bond length | 0.005 |
| RMSD bond angle | 1.400 |
| Data reduction software | HKL-2000 |
| Data scaling software | HKL-2000 |
| Phasing software | SOLVE |
| Refinement software | CNS (1.2) |
Data quality characteristics
| Overall | |
| Low resolution limit [Å] | 100.000 |
| High resolution limit [Å] | 2.000 |
| Rmerge | 0.088 |
| Number of reflections | 30364 |
| <I/σ(I)> | 18.6 |
| Completeness [%] | 100.0 |
| Redundancy | 11.2 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, HANGING DROP | 6.2 | 298 | 40% peg400, 0.1M mes, pH 6.2, VAPOR DIFFUSION, HANGING DROP, temperature 298K |
| 1 | VAPOR DIFFUSION, HANGING DROP | 6.2 | 298 | 40% peg400, 0.1M mes, pH 6.2, VAPOR DIFFUSION, HANGING DROP, temperature 298K |
