Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | APS BEAMLINE 19-BM |
| Synchrotron site | APS |
| Beamline | 19-BM |
| Temperature [K] | 100 |
| Detector technology | CCD |
| Collection date | 2009-11-05 |
| Detector | ADSC QUANTUM 210r |
| Wavelength(s) | 0.9792064 |
| Spacegroup name | P 21 21 21 |
| Unit cell lengths | 85.509, 134.026, 139.906 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 35.200 - 2.093 |
| R-factor | 0.17448 |
| Rwork | 0.174 |
| R-free | 0.19915 |
| Structure solution method | SAD |
| RMSD bond length | 0.016 |
| RMSD bond angle | 1.476 |
| Data reduction software | HKL-3000 |
| Data scaling software | HKL-3000 |
| Phasing software | MLPHARE |
| Refinement software | REFMAC (5.5.0109) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 50.000 | 2.140 |
| High resolution limit [Å] | 2.093 | 2.093 |
| Rmerge | 0.091 | 0.684 |
| Number of reflections | 94834 | |
| <I/σ(I)> | 14.5 | 2.2 |
| Completeness [%] | 99.7 | 99.7 |
| Redundancy | 5.5 | 5.3 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, SITTING DROP | 8 | 277 | 0.1 M magnesium formate, 15%(w/v) PEG3350, pH 8, VAPOR DIFFUSION, SITTING DROP, temperature 277K |
