3QX9
Crystal structure of MID domain from hAGO2 in complex with ATP
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU MICROMAX-007 HF |
Temperature [K] | 200 |
Detector technology | CCD |
Collection date | 2010-02-23 |
Detector | RIGAKU SATURN 944+ |
Spacegroup name | P 1 |
Unit cell lengths | 40.494, 46.508, 65.817 |
Unit cell angles | 87.14, 73.56, 84.56 |
Refinement procedure
Resolution | 28.700 - 2.000 |
R-factor | 0.2003 |
Rwork | 0.197 |
R-free | 0.24990 |
Structure solution method | FOURIER SYNTHESIS |
RMSD bond length | 0.016 |
RMSD bond angle | 1.577 |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Phasing software | PHENIX |
Refinement software | PHENIX ((phenix.refine: 1.5_2)) |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 28.700 |
High resolution limit [Å] | 2.000 |
Number of reflections | 26273 |
Completeness [%] | 84.8 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 8 | 277 | 0.1 M imidazole, 0.2 M NaCl, 0.46 M NaH2PO4, 1.84 M K2HPO4, VAPOR DIFFUSION, HANGING DROP, temperature 277K |