3QR2

Wild type CD147 Ig0 domain

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	ALS BEAMLINE 4.2.2
Synchrotron site	ALS
Beamline	4.2.2
Temperature [K]	100
Detector technology	CCD
Collection date	2010-12-04
Detector	NOIR-1
Wavelength(s)	1.2053
Spacegroup name	P 65 2 2
Unit cell lengths	80.257, 80.257, 160.674
Unit cell angles	90.00, 90.00, 120.00

Refinement procedure

Resolution	42.420 - 2.300
R-factor	0.2686
Rwork	0.264
R-free	0.30730
RMSD bond length	0.008
RMSD bond angle	1.098
Data reduction software	d*TREK
Data scaling software	d*TREK
Phasing software	PHENIX
Refinement software	PHENIX ((phenix.refine: 1.6.4_486))

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	42.420	2.380
High resolution limit [Å]	2.300	2.300
Number of reflections	14268
Completeness [%]		99.6

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, SITTING DROP	7	277	0.2 Na2SO4, 20% w/v PEG sulfate, pH 7, VAPOR DIFFUSION, SITTING DROP, temperature 277K