3QPT

Crystal structure of the Salmonella transcriptional regulator SlyA

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	APS BEAMLINE 21-ID-D
Synchrotron site	APS
Beamline	21-ID-D
Spacegroup name	P 65 2 2
Unit cell lengths	50.686, 50.686, 173.584
Unit cell angles	90.00, 90.00, 120.00

Refinement procedure

Resolution	39.170 - 2.400
R-factor	0.23736
Rwork	0.236
R-free	0.27126
Structure solution method	SAD
RMSD bond length	0.018
RMSD bond angle	1.771
Data reduction software	DENZO
Data scaling software	SCALEPACK
Phasing software	PHASER
Refinement software	REFMAC

Data quality characteristics

	Overall	Inner shell	Outer shell
Low resolution limit [Å]	50.000	50.000	2.240
High resolution limit [Å]	2.200	5.970	2.200
Rmerge	0.096	0.050	0.713
Number of reflections	6928
<I/σ(I)>	11.4
Completeness [%]	94.0	97.5	58.2
Redundancy	10.8	11	3.3

Crystallization Conditions

crystal ID	method	pH	temperature	details
1