3QM8
Blackfin tuna cyanomet-myoglobin, atomic resolution
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 31-ID |
Synchrotron site | APS |
Beamline | 31-ID |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2006-06-06 |
Detector | MAR CCD 165 mm |
Wavelength(s) | 0.92 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 34.318, 51.592, 38.561 |
Unit cell angles | 90.00, 104.64, 90.00 |
Refinement procedure
Resolution | 17.200 - 0.910 |
R-factor | 0.14657 |
Rwork | 0.146 |
R-free | 0.16363 |
Structure solution method | RIGID BODY refinement |
Starting model (for MR) | 2nrl |
RMSD bond length | 0.031 |
RMSD bond angle | 2.429 |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Refinement software | REFMAC (5.5.0109) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 17.200 | 0.934 |
High resolution limit [Å] | 0.910 | 0.910 |
Rmerge | 0.059 | 0.389 |
Number of reflections | 79923 | |
<I/σ(I)> | 29.9 | 3.57 |
Completeness [%] | 90.6 | 83.83 |
Redundancy | 5.5 | 4.9 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 5.6 | 0.2 M POTASSIUM/SODIUM TARTRATE, 0.1 M SODIUM CITRATE, 2.0 M AMMONIUM SULFATE, pH 5.6, VAPOR DIFFUSION, HANGING DROP |