3QAX

Crystal structure analysis of the cpb0502

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	PAL/PLS BEAMLINE 4A
Synchrotron site	PAL/PLS
Beamline	4A
Temperature [K]	100
Detector technology	CCD
Collection date	2010-04-20
Detector	ADSC QUANTUM 210
Wavelength(s)	0.99188
Spacegroup name	P 1 21 1
Unit cell lengths	40.330, 51.728, 119.694
Unit cell angles	90.00, 91.03, 90.00

Refinement procedure

Resolution	29.920 - 2.000
R-factor	0.18692
Rwork	0.184
R-free	0.25109
Structure solution method	MOLECULAR REPLACEMENT
RMSD bond length	0.022
RMSD bond angle	1.741
Data scaling software	SCALEPACK
Phasing software	CNS
Refinement software	CNS

Data quality characteristics

	Overall
Low resolution limit [Å]	29.960
High resolution limit [Å]	2.000
Number of reflections	42387
Completeness [%]	93.3

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, HANGING DROP	8	297	sodium acetate, 20% PEG 3350, 1,5-Diaminopentane dihydrochloride, pH 8.0, VAPOR DIFFUSION, HANGING DROP, temperature 297KK