3Q3S
EthR from Mycobacterium tuberculosis in complex with compound BDM5683
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | ESRF BEAMLINE ID14-2 |
| Synchrotron site | ESRF |
| Beamline | ID14-2 |
| Wavelength(s) | 0.933 |
| Spacegroup name | P 41 21 2 |
| Unit cell lengths | 121.160, 121.160, 33.820 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 19.900 - 2.000 |
| R-factor | 0.19117 |
| Rwork | 0.189 |
| R-free | 0.23150 |
| Structure solution method | MOLECULAR REPLACEMENT |
| RMSD bond length | 0.017 |
| RMSD bond angle | 1.508 |
| Refinement software | REFMAC (5.2.0019) |
Data quality characteristics
| Overall | |
| Low resolution limit [Å] | 19.900 |
| High resolution limit [Å] | 2.000 |
| Number of reflections | 17607 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, HANGING DROP | 6.5 | 293 | 0.1mM Mes pH6.5, 1.5M Ammonium Sulfate and 10% Glycerol, VAPOR DIFFUSION, HANGING DROP, temperature 293.0K |
