3PHU

OTU Domain of Crimean Congo Hemorrhagic Fever Virus

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	ESRF BEAMLINE ID14-4
Synchrotron site	ESRF
Beamline	ID14-4
Detector technology	CCD
Collection date	2009-06-21
Detector	ADSC QUANTUM 315r
Wavelength(s)	0.9795
Spacegroup name	P 32 2 1
Unit cell lengths	115.990, 115.990, 94.171
Unit cell angles	90.00, 90.00, 120.00

Refinement procedure

Resolution	49.382 - 2.200
R-factor	0.1955
Rwork	0.194
R-free	0.23110
Structure solution method	SAD
RMSD bond length	0.013
RMSD bond angle	1.488
Refinement software	PHENIX ((phenix.refine: 1.4_122))

Data quality characteristics

	Overall
Low resolution limit [Å]	50.220
High resolution limit [Å]	2.200
Number of reflections	37465

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, HANGING DROP		293	3.9M NaFormate, VAPOR DIFFUSION, HANGING DROP, temperature 293K