3PAW
Low resolution X-ray crystal structure of Yeast Rnr1p with dATP bound in the A-site
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 14-ID-B |
Synchrotron site | APS |
Beamline | 14-ID-B |
Detector technology | IMAGE PLATE |
Detector | MAR scanner 345 mm plate |
Wavelength(s) | 0.9 |
Spacegroup name | P 63 |
Unit cell lengths | 166.509, 166.509, 381.697 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 192.450 - 6.610 |
R-factor | 0.39326 |
Rwork | 0.391 |
R-free | 0.44181 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.011 |
RMSD bond angle | 1.351 |
Refinement software | REFMAC (5.5.0109) |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 192.450 |
High resolution limit [Å] | 6.610 |
Number of reflections | 9893 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 |