3PAL

IONIC INTERACTIONS WITH PARVALBUMINS. CRYSTAL STRUCTURE DETERMINATION OF PIKE 4.10 PARVALBUMIN IN FOUR DIFFERENT IONIC ENVIRONMENTS

Experimental procedure

Spacegroup name	P 41 21 2
Unit cell lengths	57.800, 57.800, 90.100
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	7.000 * - 2.400
Rwork	0.167
RMSD bond length	0.018
RMSD bond angle	3.100
Refinement software	EREF

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	9999.000 *
High resolution limit [Å]	2.400 *	2.400 *
Rmerge	0.096 *
Total number of observations	12983 *
Number of reflections	5907 *
Completeness [%]	71.0 *	57 *

Crystallization Reagents in Literatures

ID	crystal ID	solution	reagent name	concentration (unit)	details
1	1	reservoir	sodium azide	3 (mM)