3OZ0
PPAR Delta in complex with azppard02
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | SLS BEAMLINE X06SA |
| Synchrotron site | SLS |
| Beamline | X06SA |
| Temperature [K] | 100 |
| Detector technology | PIXEL |
| Collection date | 2009-09-09 |
| Detector | PSI PILATUS 6M |
| Wavelength(s) | 0.9134 |
| Spacegroup name | C 1 2 1 |
| Unit cell lengths | 113.258, 49.134, 58.574 |
| Unit cell angles | 90.00, 105.34, 90.00 |
Refinement procedure
| Resolution | 56.490 - 3.000 |
| R-factor | 0.21977 |
| Rwork | 0.215 |
| R-free | 0.27048 |
| Structure solution method | OTHER |
| Starting model (for MR) | 2gwx |
| RMSD bond length | 0.005 |
| RMSD bond angle | 0.825 |
| Data reduction software | XDS |
| Data scaling software | SCALA |
| Phasing software | MOLREP |
| Refinement software | REFMAC (5.2.0005) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 56.490 | 3.240 |
| High resolution limit [Å] | 3.000 | 3.000 |
| Rmerge | 0.098 | 0.450 |
| Number of reflections | 6381 | |
| <I/σ(I)> | 6.7 | 1.3 |
| Completeness [%] | 94.6 | 95.2 |
| Redundancy | 3 | 3 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, SITTING DROP | 8.5 | 293 | PEG, pH 8.5, VAPOR DIFFUSION, SITTING DROP, temperature 293K |
