3OEM

Crystal structure of GluN2D ligand-binding core in complex with N-methyl-D-aspartate

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	NSLS BEAMLINE X29A
Synchrotron site	NSLS
Beamline	X29A
Temperature [K]	100
Detector technology	CCD
Collection date	2007-11-15
Detector	ADSC QUANTUM 315
Wavelength(s)	1.1
Spacegroup name	C 2 2 21
Unit cell lengths	59.819, 113.885, 94.666
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	26.500 - 1.900
R-factor	0.1911
Rwork	0.189
R-free	0.22510
Structure solution method	MOLECULAR REPLACEMENT
RMSD bond length	0.006
RMSD bond angle	1.085
Refinement software	PHENIX ((phenix.refine))

Data quality characteristics

	Overall
Low resolution limit [Å]	20.000
High resolution limit [Å]	1.900
Number of reflections	25866
Completeness [%]	97.7

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, HANGING DROP			VAPOR DIFFUSION, HANGING DROP