3OEL

Crystal structure of GluN2D ligand-binding core in complex with D-glutamate

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	NSLS BEAMLINE X25
Synchrotron site	NSLS
Beamline	X25
Temperature [K]	100
Detector technology	CCD
Collection date	2008-02-20
Detector	ADSC QUANTUM 315
Wavelength(s)	1.1
Spacegroup name	C 2 2 21
Unit cell lengths	59.731, 114.195, 95.314
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	28.550 - 1.900
R-factor	0.1945
Rwork	0.193
R-free	0.22150
Structure solution method	MOLECULAR REPLACEMENT
RMSD bond length	0.005
RMSD bond angle	0.978
Refinement software	PHENIX ((phenix.refine))

Data quality characteristics

	Overall
Low resolution limit [Å]	20.000
High resolution limit [Å]	1.900
Number of reflections	25949
Completeness [%]	99.8

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, HANGING DROP			VAPOR DIFFUSION, HANGING DROP