Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | ROTATING ANODE |
| Source details | BRUKER AXS MICROSTAR |
| Temperature [K] | 113 |
| Detector technology | CCD |
| Collection date | 2009-10-05 |
| Detector | Bruker Platinum 135 |
| Wavelength(s) | 1.5418 |
| Spacegroup name | P 21 21 21 |
| Unit cell lengths | 42.360, 63.985, 82.803 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 50.630 - 1.700 |
| R-factor | 0.2313 |
| Rwork | 0.229 |
| R-free | 0.27100 |
| Structure solution method | MOLECULAR REPLACEMENT |
| RMSD bond length | 0.025 |
| RMSD bond angle | 2.028 |
| Data reduction software | SAINT |
| Data scaling software | SAINT (V7.34A) |
| Phasing software | PHASER (2.1.4) |
| Refinement software | REFMAC |
Data quality characteristics
| Overall | Inner shell | Outer shell | |
| Low resolution limit [Å] | 50.630 | 50.630 | 1.647 |
| High resolution limit [Å] | 1.690 | 3.426 | 1.590 |
| Number of reflections | 25911 | ||
| <I/σ(I)> | 166.319 | ||
| Completeness [%] | 98.6 | ||
| Redundancy | 5.24 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, HANGING DROP | 6.5 | 293 | 20% (w/v) PEG 3350, 0.1M Tris-HCl, 0.2M sodium acetate pH 7.5, 0.02% azide, VAPOR DIFFUSION, HANGING DROP, temperature 293K |
